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氫氧化鉀的質(zhì)量指標(biāo)可從哪些方面檢測(cè)出

發(fā)布來(lái)源:http://m.51fww.cn    更新時(shí)間:2022-12-16 點(diǎn)擊數(shù):100

 
氫氧化鉀相信大家都不陌生了吧,那么它的質(zhì)量指標(biāo)是什么呢?接下來(lái)跟隨小編一起簡(jiǎn)單了解一下吧。
It is believed that everyone is familiar with potassium hydroxide. What is its quality index? Let's follow Xiao Bian to have a brief understanding.
1、水不溶物:5%氫氧化鉀試樣水溶液應(yīng)無(wú)色透明。
1. Water insoluble matter: 5% potassium hydroxide sample aqueous solution shall be colorless and transparent.
2、鉛:取試樣1g溶于5ml水和11ml稀鹽酸試液的混合液中,冷卻。以此作為試樣液按GT-18方法測(cè)定。對(duì)照液中的鉛離子量取10μg。
2. Lead: Dissolve 1g of sample in 5ml water and 11ml dilute hydrochloric acid test solution, and cool it. Take this as the sample solution and determine according to GT-18 method. The amount of lead ion in the control solution is 10 μ g。
3、碳酸鹽:在含量分析中介于酚酞和甲基橙終點(diǎn)之間所耗的每mL1mol/L硫酸,相當(dāng)于碳酸鉀138、2mg。
3. Carbonate: every mL1mol/L of sulfuric acid consumed between the end points of phenolphthalein and methyl orange in content analysis is equivalent to 138 and 2mg of potassium carbonate.
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4、重金屬:取試樣670mg,溶于5ml水和5ml稀鹽酸試液(TS-117)的混合液中。加熱沸,冷卻,用水稀釋25ml,后過(guò)濾。以此作為試樣液,按GT-16方法測(cè)定。用含20μg鉛離子的對(duì)照液(溶液A)。
4. Heavy metal: take 670mg sample and dissolve it in 5ml water and 5ml dilute hydrochloric acid test solution (TS-117). Heat to boiling, cool, dilute with water to 25ml, and filter. Take this as the sample solution, and determine according to GT-16 method. 20 for use μ G Reference solution of lead ion (solution A).
5、汞:按CT-22方法測(cè)定。標(biāo)準(zhǔn)液和試樣液按如下方法制備。
5. Mercury: determined according to CT-22 method. The standard solution and sample solution shall be prepared as follows.
(1)標(biāo)準(zhǔn)液的制備:按GT-22制各貯液和稀釋液,使所得溶液每ml中含汞1μg。取該溶液1ml,放入-50ml燒杯,加水20ml.1:4稀硫酸溶液1ml和4%高錳酸鉀溶液1ml。用表面皿蓋住燒杯,煮沸數(shù)秒鐘后冷卻,備用。
(1) Preparation of standard solution: prepare each storage solution and diluent according to GT-22, so that each ml of the obtained solution contains 1 mercury μ g。 Take 1ml of the solution, put it into a - 50ml beaker, and add 20ml of water 1: 4 Dilute sulfuric acid solution 1ml and 4% potassium permanganate solution 1ml. Cover the beaker with a watch glass, boil it for a few seconds, and then cool it for standby.
(2)試樣液的制備:取試樣10.0g放入-100ml燒杯,加水15ml使之溶解,加酚酞試液(TS-167)2滴,在不斷攪拌下用1:1稀鹽酸溶液緩慢中和。加1:稀硫酸溶液1ml和4%高錳酸鉀溶液1ml,用表面皿蓋住燒杯,煮沸數(shù)秒鐘后冷卻,備用。
(2) Preparation of sample solution: put 10.0g of sample into a 100ml beaker, add 15ml of water to dissolve it, add 2 drops of phenolphthalein test solution (TS-167), and slowly neutralize it with 1:1 dilute hydrochloric acid solution under constant stirring. Add 1ml of 1: dilute sulfuric acid solution and 1ml of 4% potassium permanganate solution, cover the beaker with a watch glass, boil for a few seconds, and then cool down for standby.
以上關(guān)于氫氧化鉀的質(zhì)量指標(biāo)就為大家簡(jiǎn)單介紹到這里了,如果您還有什么不明的地方就請(qǐng)直接來(lái)聯(lián)系我們http://m.51fww.cn吧。
The above quality indicators of potassium hydroxide will be briefly introduced here. If you have anything unclear, please contact us directly http://m.51fww.cn Right.

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